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ACTINIS - 带屏蔽功能的IMS

用于分析放射性样品的高性能屏蔽式 SIMS 仪器
众所周知,动态二次离子质谱仪(SIMS)适用于广泛的核科学应用,但对于高放射性材料(如辐照核燃料)的研究,则需要使用特定的仪器。
ACTINIS 源于经过实证的 CAMECA IMS 7f 系统,设计用于在安全环境中对放射性样品进行高精度元素和同位素分析:它集成在一套生物保护装置中,以保护操作人员在样品转移和分析过程中免受污染和辐照影响,并配有多个用于最大限度地减少人工操作的特殊装置(如安全进样系统)。
  • 产品概述 +


    划时代的 SIMS 性能
    ACTINIS 保留了 IMS 7f/7f-GEO 型号的最佳特性,可提供高灵敏度的深度剖析和同位素比测量,以及亚微米级横向分辨率的元素和同位素图谱。
    • 双等离子体和铯一次离子源的组合,确保了对正电和负电物质有最佳的灵敏度
    • 二次离子光学收集系统具有高电场,可优化传输,还有光束对中,可实现优异的重复性,其光学选通功能还可实现高动态范围的深度剖析
    • 双聚焦质谱仪(用于能量聚焦的静电分析仪,具有快速峰值切换功能的叠层磁铁)
    • 带有一个电子倍增器(EM)和两个法拉第杯(FC)的特殊检测系统,采用最先进的测电技术(低噪声和稳定的基线)
    • 用于仪器调谐的直接离子成像
    • 扫描离子成像,用于以高横向分辨率绘制大小区域的图谱。

    最先进的屏蔽技术

    包装中包含机械图纸和生物保护装置(仪器屏蔽装置)的详细规格,确保了辐射安全以及轻松与 SIMS 仪器进行连接。ACTINIS 配备了足够的手套箱(阿尔法保护)和铅壁室(伽马保护),可以分析在距离样品 5 厘米处测得的活性(剂量率)高达 2 Gy/h 的样品。

    全自动和易于使用
    ACTINIS 的自动化水平高,配有多个用于最大限度地减少人工操作的特殊装置,如安全进样系统等。我们开发了特殊工具,并对离子光学装置进行了改进,现在用户能够轻松在屏蔽装置内部进行维护。

    ACTINIS™ 的灵感来自于希腊语“ἀκτίς”(射线),同时也指核应用中特别重要的化学元素,即锕系元素。
  • Download documentation +

  • 科学出版物 +


    Below is a selection of research articles by users of CAMECA Shielded IMS

    You are welcome to send us any missing references, pdf and supplements! Please email cameca.info@ametek.com.

    SIMS analysis of irradiated HTR fuel. S. Brémier, M. Laurie, R. Hasnaoui and A. El Abjani (2015), SIMS XX Poster Presentation, Sept. 13-18, 2015.

    Evidence of tellurium iodide compounds in apower-ramped irradiated UO2 fuel rod. L. Desgranges, Ch. Riglet-Martial, I. Aubrun, B. Pasquet, I. Roure, J. Lamontagne, T. Blay (2013), Journ al of Nuclear Materia ls, Volume 437, Issue 1-3, Pages 409-414. doi:10.1016/j.jnucmat.2013.02.059.

    Measurement of energy spectra on irradiated polycrystalline UO2 samples using secondary ion mass spectrometry. I. Roure, B. Pasquet, L. Desgranges, Ph. Bienvenu (2012), Surface and Interface Analysis, Volume 45, Issue 1, Pages 427-429. DOI: 10.1002/sia.5115.

    Microbeam analysis of irradiated nuclear fuel. C T Walker, S Brémier, P Pöml, D Papaioannou, P W D Bottomley (2012), EMAS 2011: 12th European Workshop on Modern Developments in Microbeam Analysis, IOP Conf. Series: Materials Science and Engineering, Volume 32, 012028. doi:10.1088/1757-899X/32/1/012028.

    High burnup changes in UO2 fuels irradiated up to 83 GWD/T in M5® claddings. J. Noirot, I. Aubrun, L. Desgranges, K. Hanifi, J. Lamontagne, B. Pasquet, C. Valot, P. Blanpain, H. Cognon (2009), Nuclear Engineering and Technology, Volume 41, No.2, March 2009 – Special Issue on the Water Reactor Fuel Performance Meeting 2008.

    SIMS characterisation of actinide isotopes in irradiated nuclear fuel. L. Desgranges, B. Pasquet, Ch. Valot, I. Roure (2009), Journal of Nuclear Materials, Proceedings of a Topical Conference on Plutonium and Actinides: Plutonium Futures - The Science 2008, Volume 385, Issue 1, Pages 99-102. doi:10.1016/j.jnucmat.2008.09.032.

    SIMS analysis of an UO2 fuel irradiated at low temperature to 65 MWd/kgHM. C.T. Walker, S. Bremier, S. Portier, R. Hasnaoui, W. Goll (2009). Journal of Nuclear Materials, Volume 393, Issue 2, Pages 212-223. doi:10.1016/j.jnucmat.2009.06.017.

    Investigation of the relative sensitivity factor for the quantification of ion microprobe results for Nd isotopes in simulated nuclear fuel. Stéphane Portier, Stéphane Brémier, Rachid Hasnaoui, Olivier Bildstein, Clive T. Walker (2008), Microchimica Acta, Volume 161, Issue 3-4, Pages 479-483. DOI10.1007/s00604-007-0895-8.

    A method for the quantification of total xenon concentration in irradiated nuclear fuel with SIMS and EPMA. Lionel Desgranges, Christophe Valot, Bertrand Pasquet, Jérôme Lamontagne, Thierry Blay, Ingrid Roure (2008), Nuclear Instruments and Methods in Physics Research B: Beam Interactions with Materials and Atoms, Volume 266, Issue 1, Pages 147-154. doi:10.1016/j.nimb.2007.10.035.

    Assessment of the Nd/U ratio for the quantification of neodymium in UO2. L. Desgranges, B. Pasquet, I. Roure, S. Portier, S. Brémier, C.T.Walker, R. Hasnaoui, D. Gavillet, M. Martin, L. Raimbault (2008), Applied Surface Science, Volume 255, Issue 4, Pages 863-865. doi:10.1016/j.apsusc.2008.05.196.

    Detailed characterisations of high burn-up structures in oxide fuels. J. Noirot, L. Desgranges, J. Lamontagne (2008), Journal of Nuclear Materials, Volume 372, Issues 2-3, Pages 318-339. doi:10.1016/j.jnucmat.2007.04.037.

    Study of structural material resulting from the nuclear fuel cycle using SEM-WDX, EPMA and SIMS techniques. Jérôme Lamontagne, Catherine Eysseric, Lionel Desgranges, Christophe Valot, Jean Noirot, Thierry Blay, Ingrid Roure, Bertrand Pasquet (2008), Microchimica Acta, Volume 161, Issue 3, Pages 355-362. DOI10.1007/s00604-007-0852-6.

    SIMS analysis of 83Kr implanted UO2. S. Portier, S. Brémier, R. Hasnaoui, O. Bildstein, C.T. Walker (2008), Applied Surface Science, Volume 255, Issue 4, Pages 1323-1326. doi:10.1016/j.apsusc.2008.05.263.

    Secondary ion mass spectrometry of irradiated nuclear fuel and cladding: An overview. S. Portier, S. Brémier, C.T. Walker (2007). International Journal of Mass Spectrometry, Volume 263, Issues 2-3, Pages 113-126. doi:10.1016/j.ijms.2007.01.016.

    Fission Gas Bubbles Characterisation in Irradiated UO2 Fuel by SEM, EPMA and SIMS. Jérôme Lamontagne, Lionel Desgranges, Christophe Valot, Jean Noirot, Thierry Blay, Ingrid Roure, Bertrand Pasquet (2006), Microchimica Acta, Volume 155, Pages 183-187. DOI 10.1007/s00604-006-0540-y.

    Installation of a Shielded SIMS for the Analysis of Irradiated Nuclear Fuels. Stéphane Brémier, Rachid Hasnaoui, Stéphane Portier, Olivier Bildstein, and Clive T. Walker. (2006), Microchimica Acta, Volume 155, Pages 113-120. DOI 10.1007/s00604-006-0527-8.

    A shielded SIMS in CEA : a new tool for the low abundant isotopes characterization. L.Desgranges, B.Pasquet (2005), ATALANTE 2004, P2-17.
    Characterisation of irradiated nuclear fuel with SIMS. L. Desgranges, Ch.Valot, B.Pasquet (2005), Applied Surface Science, Volume 252, Issue 19, Pages 7048-7050. doi:10.1016/j.apsusc.2006.02.256.

    Detection of Gas Bubble by SIMS in Irradiated Nuclear Fuel. Jérôme Lamontagne, Jean Noirot, Lionel Desgranges, Thierry Blay, Bertrand Pasquet, Ingrid Roure (2004), Microchimica Acta, Volume 145, Issue 1, Pages 91-94. DOI 10.1007/s00604-003-0135-9.

    Measurement of xenon in uranium dioxide (UO2) with SIMS. L. Desgranges, B. Pasquet (2004), Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms. Volume 215, Issues 3-4, Pages 545-551. doi:10.1016/j.nimb.2003.08.033.

    A new shielded SIMS instrument for analysis of highly radioactive materials.
    B. Rasser, L, Desgranges, B. Pasquet (2003), Applied Surface Science, Secondary ion mass spectrometry SIMS XIII, Volume 203-204, Pages 673-678. doi:10.1016/S0169-4332(02)00789-4.

    One Year of Operation of the Shielded SIMS with Irradiated Materials in the LECA Facility. L.Desgranges, B.Pasquet (2003), Proceedings of the Plenary Meeting 2003, European Working Group " Hot Laboratories and Remote Handling".

    Installation of a shielded SIMS in CEA Cadarache. L. Desgranges, B. Pasquet, B. Rasser (2001).